benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

Base Information

Chemical Name:benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate
CAS No.:1017279-80-9
Molecular Formula:C₁₉H₂₇NO₄
Molecular Weight:333.428
Hs Code.:

Synonyms:benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

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Chemical Property of benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

Chemical Property:

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Technology Process of benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

There total 4 articles about benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1017279-67-2
tert-butyl (1S,3R)-3-azidocarbonyl-2,2-dimethylcyclobutane-1-carboxylate

: 100-51-6,185532-71-2
benzyl alcohol

: 1017279-80-9
benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

Guidance literature:: In toluene; Heating;
DOI:10.1016/j.tetasy.2008.01.020

Reference yield:

: 288848-24-8
(1S,3R)-3-acetyl-2,2-dimethylcyclobutane carboxylic acid

: 1017279-80-9
benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 0 °C

2.1: sodium hypobromide / 1,4-dioxane; water

3.3: Reflux

With dmap; sodium hypobromide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; water;
DOI:10.1007/s00726-011-0912-4

Reference yield:

: 80-57-9,1196-01-6
(-)-Verbenone

: 1017279-80-9
benzyl (1R,3S)-3-tert-butoxycarbonyl-2,2-dimethylcyclobutyl-1-carbamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium periodate; ruthenium trichloride / dichloromethane; water; acetonitrile / 20 °C

2.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / tetrahydrofuran / 0 °C

3.1: sodium hypobromide / 1,4-dioxane; water

4.3: Reflux

With dmap; ruthenium trichloride; sodium periodate; sodium hypobromide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile;
DOI:10.1007/s00726-011-0912-4