N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

Base Information

Chemical Name:N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide
CAS No.:109364-24-1
Molecular Formula:C₅₂H₅₄N₆O₈
Molecular Weight:891.036
Hs Code.:

Synonyms:N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

Suppliers and Price of N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

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Technology Process of N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

There total 3 articles about N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35737-15-6
Fmoc-Trp-OH

: 109364-24-1
N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / dimethylformamide / 0.08 h / -20 °C

2: dimethylformamide / 1 h / Ambient temperature

With 4-methyl-morpholine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00391a017

Reference yield:

: 65864-24-6
Boc-Nle-Asp(OBzl)-Phe-NH₂

: 109364-24-1
N-(((fluorenylmethyl)oxy)carbonyl)-L-tryptophyl-L-norleucyl-L-(β-benzyl-L-aspartyl)henylalanine amide

Guidance literature:: Multi-step reaction with 2 steps

1: TFA / 0.5 h

2: dimethylformamide / 1 h / Ambient temperature

With trifluoroacetic acid; In N,N-dimethyl-formamide;
DOI:10.1021/jm00391a017