(R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide

Base Information

• Chemical Name: (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide
• CAS No.: 956599-29-4
• Molecular Formula: C₁₅H₂₁NO₅
• Molecular Weight: 295.335

Synonyms:(R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide

Chemical Property of (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide

There total 2 articles about (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

(R,S)-4-nitro-3-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)-phenol (956599-27-2) + acetic anhydride (108-24-7) → (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide (956599-29-4)

Guidance literature:

With hydrogen; 5%-palladium/activated carbon; In Isopropyl acetate; at 20 - 25 ℃; under 3000.3 Torr;

Reference yield:

(R,S)-4-amino-3-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)-phenol (956599-28-3) + 4-amino-2-chloro-5-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)phenol (1056941-47-9) + acetic anhydride (108-24-7) → (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide (956599-29-4) + N-[5-chloro-4-hydroxy-2-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)phenyl]acetamide (956599-38-5)

Guidance literature:

In ethyl acetate; at 20 - 25 ℃; for 1.5h; Product distribution / selectivity;

Reference yield: 44.0%

(R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide (956599-29-4) → N-[2-(2,3-dihydroxy-2-methyl-propoxy)-4-hydroxy-phenyl]-acetamide (956599-31-8)

Guidance literature:

With hydrogenchloride; water; In 2-methyltetrahydrofuran; at 20 ℃;

upstream raw materials:

(R,S)-4-nitro-3-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)-phenol

acetic anhydride

(R,S)-4-amino-3-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)-phenol

4-amino-2-chloro-5-(2,2,4-trimethyl-[1,3]dioxolan-4-ylmethoxy)phenol

Downstream raw materials:

N-[2-(2,3-dihydroxy-2-methyl-propoxy)-4-hydroxy-phenyl]-acetamide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 956599-29-4 (R,S)-N-[4-hydroxy-2-(2,2,4-trimethyI-[1,3]dioxolan-4-ylmethoxy)-phenyl]-acetamide

Send

Send

Metric Ton KG G Pound L ML

Send

Send