4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid

Base Information

• Chemical Name: 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid
• CAS No.: 1040380-20-8
• Molecular Formula: C₂₈H₄₄N₄O₈SSi
• Molecular Weight: 624.831

Synonyms:4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid

Chemical Property of 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid

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Technology Process of 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid

There total 1 articles about 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

methyl 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyrate (1040380-19-5) → 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid (1040380-20-8)

Guidance literature:

With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 16h;

DOI:10.1055/s-2008-1066982

Reference yield:

4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid (1040380-20-8) + CbzGlyGly (2566-19-0) → 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-[N-(benzyloxycarbonyl)-glycyl-glycyl]-2,6-dideoxy-α-D-galactopyranosyl)sulfanyl]butyramide (1040380-66-2)

Guidance literature:

Multistep reaction.;

DOI:10.1055/s-2008-1066982

Reference yield:

C10H10N2O3 + 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyric acid (1040380-20-8) → 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-2,6-dideoxy-3-O-[(4-ethoxyphenyl)carbamoyl]-α-D-galactopyranosyl)sulfanyl]butyramide (1040380-40-2)

Guidance literature:

Multistep reaction.;

DOI:10.1055/s-2008-1066982

upstream raw materials:

methyl 4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-(tert-butyldimethylsilyl)-2,6-dideoxy-4-O-(4-methoxybenzyl)-α-D-galactopyranosyl)sulfanyl]butyrate

Downstream raw materials:

4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-2,6-dideoxy-3-O-[(4-fluorophenyl)carbamoyl]-α-D-galactopyranosyl)sulfanyl]butyramide

4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-2,6-dideoxy-4-O-[(4-fluorophenyl)carbamoyl]-α-D-galactopyranosyl)sulfanyl]butyramide

4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-3-O-[(4-cyanophenyl)carbamoyl]-2,6-dideoxy-α-D-galactopyranosyl)sulfanyl]butyramide

4-[(2-{[(allyloxy)carbonyl]amino}-6-azido-4-O-[(4-cyanophenyl)carbamoyl]-2,6-dideoxy-α-D-galactopyranosyl)sulfanyl]butyramide

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