2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane

Base Information

• Chemical Name: 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane
• CAS No.: 73652-50-3
• Molecular Formula: C₃₉H₄₉N₁₁O₁₂
• Molecular Weight: 863.885

Synonyms:2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane

Chemical Property of 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane

Chemical Property:

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Technology Process of 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane

There total 6 articles about 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N⁶-yl)butane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

N6-(4-aminobutyl)-2',3'-O-(methoxyethylidene)adenosine (73644-56-1) + 9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine (73644-54-9) → 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N6-yl)butane (73652-50-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

DOI:10.1021/jm00181a015

Reference yield: 40.0%

6-chloro-9-<2,3-O-(methoxyethylidene)-β-D-ribofuranosyl>purine (73644-53-8) + 2',3'-O-<<methyl>ethoxymethylidene>-N6-(4-aminobutyl)adenosine (73644-55-0) → 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N6-yl)butane (73652-50-3)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 18h; Ambient temperature;

DOI:10.1021/jm00181a015

Reference yield:

6-Chloropurine riboside (2004-06-0) → 2',3'-O-<<methyl>ethoxymethylidene>-2,3-O-(methoxyethylidene)-1,4-di(adenosin-N6-yl)butane (73652-50-3)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl / dimethylformamide / Ambient temperature

2: 40 percent / Et₃N / dimethylformamide / 18 h / Ambient temperature

With hydrogenchloride; triethylamine; In N,N-dimethyl-formamide;

DOI:10.1021/jm00181a015

upstream raw materials:

6-chloro-9-<2,3-O-(methoxyethylidene)-β-D-ribofuranosyl>purine

2',3'-O-<<methyl>ethoxymethylidene>-N⁶-(4-aminobutyl)adenosine

N⁶-(4-aminobutyl)-2',3'-O-(methoxyethylidene)adenosine

9-<2',3'-O-<<methyl>ethoxymethylidene>-β-D-ribofuranosyl>-6-chloropurine

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