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4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester

Base Information
  • Chemical Name:4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester
  • CAS No.:271786-19-7
  • Molecular Formula:C17H24O5
  • Molecular Weight:308.375
  • Hs Code.:
4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester

Synonyms:4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester

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Chemical Property of 4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester
Chemical Property:
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Technology Process of 4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester

There total 2 articles about 4-methoxycarbonyloxybenzoic acid (S)-1-methylheptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 96 percent / sodium hydroxide / H2O
2: 94 percent / triphenylphosphine; diethyl azodicarboxylate / tetrahydrofuran / 48 h / 20 °C
With sodium hydroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water;
DOI:10.1002/anie.200603053
Guidance literature:
Multi-step reaction with 2 steps
1: 49 percent / NaOH / H2O / 0.5 h / 4 °C
2: 73 percent / diethyl azodicarboxylate, PPh3 / diethyl ether / 50 h / Ambient temperature
With sodium hydroxide; triphenylphosphine; diethylazodicarboxylate; In diethyl ether; water;
DOI:10.1246/cl.1996.583
Guidance literature:
With ammonium hydroxide; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1002/anie.200603053
upstream raw materials:

4-hydroxy-benzoic acid

Downstream raw materials:

4-hydroxybenzoic acid (S)-1-methylheptyl ester

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