C₃₉H₇₁NO₆S₂Si₂

Base Information

Chemical Name:C₃₉H₇₁NO₆S₂Si₂
CAS No.:1591927-28-4
Molecular Formula:C₃₉H₇₁NO₆S₂Si₂
Molecular Weight:770.299
Hs Code.:

C<sub>39</sub>H<sub>71</sub>NO<sub>6</sub>S<sub>2</sub>Si<sub>2</sub>

Synonyms:C₃₉H₇₁NO₆S₂Si₂

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Chemical Property of C₃₉H₇₁NO₆S₂Si₂

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Technology Process of C₃₉H₇₁NO₆S₂Si₂

There total 12 articles about C₃₉H₇₁NO₆S₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1591927-96-6
C₃₃H₅₇NO₆S₂Si

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1591927-28-4
C₃₉H₇₁NO₆S₂Si₂

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-46-6
C₁₅H₃₄O₂Si₂

: 1591927-28-4
C₃₉H₇₁NO₆S₂Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / -95 - -78 °C / Inert atmosphere

2.1: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

3.1: camphor-10-sulfonic acid / dichloromethane; methanol / 4 h / 0 - 20 °C / Inert atmosphere

4.1: camphor-10-sulfonic acid / dichloromethane; methanol / 2 h / 0 °C / Inert atmosphere

5.1: Proton-sponge / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

6.1: diisobutylaluminium hydride / dichloromethane; toluene / -10 °C / Inert atmosphere

7.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

9.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

10.1: tin(II) trifluoromethanesulfonate; 1-ethyl-piperidine / dichloromethane / 4.5 h / -50 °C / Inert atmosphere

10.2: 12 h / -78 °C / Inert atmosphere

11.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With 1-ethyl-piperidine; 2,6-dimethylpyridine; dmap; tin(II) trifluoromethanesulfonate; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; toluene; acetonitrile; tert-butyl alcohol; 1.1: |Mukaiyama Aldol Addition;
DOI:10.1021/ol5008179

Reference yield:

: 1591927-49-9
C₃₂H₅₂O₄Si₂

: 1591927-28-4
C₃₉H₇₁NO₆S₂Si₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: tetramethylammonium triacetoxyborohydride / acetonitrile; acetic acid / 24 h / -40 - -30 °C / Inert atmosphere

2.1: camphor-10-sulfonic acid / dichloromethane; methanol / 4 h / 0 - 20 °C / Inert atmosphere

3.1: camphor-10-sulfonic acid / dichloromethane; methanol / 2 h / 0 °C / Inert atmosphere

4.1: Proton-sponge / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

5.1: diisobutylaluminium hydride / dichloromethane; toluene / -10 °C / Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

8.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

9.1: tin(II) trifluoromethanesulfonate; 1-ethyl-piperidine / dichloromethane / 4.5 h / -50 °C / Inert atmosphere

9.2: 12 h / -78 °C / Inert atmosphere

10.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

With 1-ethyl-piperidine; 2,6-dimethylpyridine; dmap; tin(II) trifluoromethanesulfonate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; Dess-Martin periodane; triethylamine; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; dichloromethane; acetic acid; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/ol5008179