N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide

Base Information

• Chemical Name: N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide
• CAS No.: 1173713-20-6
• Molecular Formula: C₁₀H₉BrN₄O₂
• Molecular Weight: 297.111
• Mol file: 1173713-20-6.mol

Synonyms:N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide

Chemical Property of N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide

There total 1 articles about N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-Amino-5-bromo-4-nitrobenzonitrile (1173713-52-4) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide (1173713-20-6)

Guidance literature:

for 0.333333h;

Reference yield: 60.0%

N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide (1173713-20-6) → N'-(5-amino-4-bromo-2-cyanophenyl)-N,N-dimethylformimidamide (1173713-21-7)

Guidance literature:

N'-(4-bromo-2-cyano-5-nitrophenyl)-N,N-dimethylformimidamide; With hydrogenchloride; titanium(III) chloride; In tetrahydrofuran; water; at 0 - 20 ℃; for 4h;

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; pH=9;

upstream raw materials:

2-Amino-5-bromo-4-nitrobenzonitrile

N,N-dimethyl-formamide dimethyl acetal

Downstream raw materials:

N'-(5-amino-4-bromo-2-cyanophenyl)-N,N-dimethylformimidamide