C₃₅H₄₈O₅Si

Base Information

Chemical Name:C₃₅H₄₈O₅Si
CAS No.:1286242-08-7
Molecular Formula:C₃₅H₄₈O₅Si
Molecular Weight:576.849
Hs Code.:

C<sub>35</sub>H<sub>48</sub>O<sub>5</sub>Si

Synonyms:C₃₅H₄₈O₅Si

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Chemical Property of C₃₅H₄₈O₅Si

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Technology Process of C₃₅H₄₈O₅Si

There total 13 articles about C₃₅H₄₈O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1286242-07-6
C₃₄H₄₄O₅Si

: 917-54-4
methyllithium

: 1286242-08-7
C₃₅H₄₈O₅Si

Guidance literature:: With copper(l) cyanide; In diethyl ether; at -50 - -30 ℃; regioselective reaction;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-97-1
C₃₀H₄₈O₄Si₂

: 1286242-08-7
C₃₅H₄₈O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1: Dess-Martin periodane / dichloromethane

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

3: trimethylaluminum / dichloromethane; water / -50 °C

4: toluene-4-sulfonic acid / benzene / Reflux

5: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

6: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

7: copper(l) cyanide / diethyl ether / -50 - -30 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene; 1: Dess-Martin oxidation / 1: Wittig reaction / 6: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106

Reference yield:

: 1286241-95-9
C₃₀H₄₈O₃Si₂

: 1286242-08-7
C₃₅H₄₈O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

2: Dess-Martin periodane / dichloromethane

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran; water

4: trimethylaluminum / dichloromethane; water / -50 °C

5: toluene-4-sulfonic acid / benzene / Reflux

6: diisobutylaluminium hydride / tetrahydrofuran / 0 °C

7: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -30 °C

8: copper(l) cyanide / diethyl ether / -50 - -30 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; trimethylaluminum; copper(l) cyanide; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; benzene; 1: Katsuki-Sharpless epoxidation / 2: Dess-Martin oxidation / 2: Wittig reaction / 7: Katsuki-Sharpless epoxidation;
DOI:10.3987/COM-10-12106