1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

Base Information

Chemical Name:1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine
CAS No.:1454854-84-2
Molecular Formula:C₂₄H₃₁N₅
Molecular Weight:389.544
Hs Code.:

Synonyms:1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

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Chemical Property of 1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

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Technology Process of 1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

There total 3 articles about 1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 766-47-2
1-ethynyl-2-methylbenzene

: 1-(3-azidopropyl)-4-(3,4-dimethylphenyl)piperazine

: 1454854-84-2
1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

Guidance literature:: With copper nanoparticles on activated carbon; In 1,4-dioxane; at 60 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

: 1454858-00-4
C₁₂H₁₃N₃O

: 1014-05-7
1-(3,4-dimethylphenyl)piperazine

: 1454854-84-2
1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

Guidance literature:: C₁₂H₁₃N₃O; 1-(3,4-dimethylphenyl)piperazine; In dichloromethane; at 20 ℃; for 0.166667h;

With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.5h; Molecular sieve;

With sodium tris(acetoxy)borohydride; for 12h;
DOI:10.5012/bkcs.2013.34.11.3467

Reference yield:

: 1454857-88-5
3-(4-o-tolyl-1H-1,2,3-triazole-1-yl)propan-1-ol

: 1454854-84-2
1-(3,4-dimethylphenyl)-4-(3-(4-(o-tolyl)-1H-1,2,3-triazol-1-yl)propyl)piperazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl dichloride; dimethylsulfone / dichloromethane / 0.5 h / -78 °C

1.2: 1.08 h / -78 - 20 °C

2.1: dichloromethane / 0.17 h / 20 °C

2.2: 0.5 h / Molecular sieve

2.3: 12 h

With oxalyl dichloride; dimethylsulfone; In dichloromethane;
DOI:10.5012/bkcs.2013.34.11.3467