6-methoxy-2-methyl-3-nitrobenzylidene diacetate

Base Information

Chemical Name:6-methoxy-2-methyl-3-nitrobenzylidene diacetate
CAS No.:474454-38-1
Molecular Formula:C₁₃H₁₅NO₇
Molecular Weight:297.265
Hs Code.:

Synonyms:6-methoxy-2-methyl-3-nitrobenzylidene diacetate

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Chemical Property of 6-methoxy-2-methyl-3-nitrobenzylidene diacetate

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Technology Process of 6-methoxy-2-methyl-3-nitrobenzylidene diacetate

There total 1 articles about 6-methoxy-2-methyl-3-nitrobenzylidene diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 81029-03-0
4-Methoxy-2,3-dimethylnitrobenzene

: 108-24-7
acetic anhydride

: 474454-40-5
6-methoxy-2-methyl-3-nitrobenzyl acetate

: 474454-38-1
6-methoxy-2-methyl-3-nitrobenzylidene diacetate

Guidance literature:: With chromium(VI) oxide; sulfuric acid; In acetic acid; at 5 - 10 ℃; for 2h;
DOI:10.1021/jm0202270

Reference yield: 96.0%

: 474454-38-1
6-methoxy-2-methyl-3-nitrobenzylidene diacetate

: 474454-42-7
6-methoxy-2-methyl-3-nitrobenzaldehyde

Guidance literature:: With sulfuric acid; In ethanol; for 2h; Heating;
DOI:10.1021/jm0202270

Reference yield:

: 474454-38-1
6-methoxy-2-methyl-3-nitrobenzylidene diacetate

: 4-{[1-(2,5-Dihydroxy-phenyl)-meth-(E)-ylidene]-amino}-7-hydroxy-2-phenethyl-2,3-dihydro-isoindol-1-one

Guidance literature:: Multi-step reaction with 8 steps

1: 96 percent / H₂SO₄ / aq. ethanol / 2 h / Heating

2: 84 percent / KMnO₄; NaOH / H₂O / 2 h / Heating

3: 95 percent / methanol; hexane / 0.5 h / 20 °C

4: 53 percent / N-bromosuccinimide; dibenzoyl peroxide / CCl₄ / 13 h / Heating

5: 93 percent / triethylamine / methanol / 24 h / 80 °C

6: 88 percent / BBr₃ / CH₂Cl₂ / 2 h / 0 - 10 °C

7: 90 percent / H₂ / Pd/C/50 percent water / methanol / 0.5 h / 20 °C / atmospheric pressure

8: methanol / 6 h / Heating

With sodium hydroxide; potassium permanganate; N-Bromosuccinimide; sulfuric acid; hydrogen; boron tribromide; triethylamine; dibenzoyl peroxide; palladium on activated charcoal; water; In methanol; tetrachloromethane; ethanol; hexane; dichloromethane; water; 4: Wohl-Ziegler conditions;
DOI:10.1021/jm0202270