13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

Base Information

Chemical Name:13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam
CAS No.:91652-55-0
Molecular Formula:C₃₉H₆₁N₃O₅S₄
Molecular Weight:780.194
Hs Code.:

Synonyms:13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

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Technology Process of 13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

There total 5 articles about 13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 91652-53-8
13-Oxo-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

: 540-63-6
ethane-1,2-dithiol

: 91652-55-0
13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

Guidance literature:: With methanol; boron trifluoride; In acetic acid; at 20 ℃; for 20h;
DOI:10.1002/hlca.19840670819

Reference yield:

: 91653-21-3
13-Nitro-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

: 91652-55-0
13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOMe, 2.) TiCl₃, NaOAc / 1.) MeOH, 20 deg C, 10 min, 2.) MeOH, H₂O, 20 deg C, 16 h

2: 98 percent / BF₃/MeOH / acetic acid / 20 h / 20 °C

With methanol; titanium(III) chloride; boron trifluoride; sodium methylate; sodium acetate; In acetic acid;
DOI:10.1002/hlca.19840670819

Reference yield:

: 4748-73-6
N-(cyanoethyl)-1,4-diaminobutane

: 91652-55-0
13,13-(Aethylendithio)-N-<4-tosyl-8-(tosylamino)-4-azaoctyl>-16-hexadecanlactam

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / K₂CO₃

2: 62 percent / NaBH₄/CoCl₂

3: NaCNBH₃

4: 1.) NaOMe; 2.) TiCl₃/AcONH₄ / 1.)MeOH; 2.) H₂O

5: 10percent BF₃ / methanol

With sodium tetrahydroborate; titanium(III) chloride; boron trifluoride; ammonium acetate; sodium methylate; sodium cyanoborohydride; potassium carbonate; In methanol;
DOI:10.1016/S0040-4039(01)80211-2