Technology Process of C17H18N4O4
There total 5 articles about C17H18N4O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium carbonate;
In
water; acetonitrile;
at 100 ℃;
for 3h;
Inert atmosphere;
DOI:10.1016/j.bmc.2012.07.003
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / ethanol / 1.5 h / 0 °C
2: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C
3: sodium carbonate; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine / acetonitrile; water / 3 h / 100 °C / Inert atmosphere
With
sodium tetrahydroborate; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; sodium carbonate; triethylamine tris(hydrogen fluoride);
In
tetrahydrofuran; ethanol; water; acetonitrile;
3: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.07.003
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridine / 4 h / 20 °C
2: pyridine; chromium(VI) oxide; acetic anhydride / 1.5 h / 0 °C
3: sodium tetrahydroborate / ethanol / 1.5 h / 0 °C
4: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 °C
5: sodium carbonate; palladium diacetate; trisodium tris(3-sulfophenyl)phosphine / acetonitrile; water / 3 h / 100 °C / Inert atmosphere
With
pyridine; chromium(VI) oxide; sodium tetrahydroborate; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; acetic anhydride; sodium carbonate; triethylamine tris(hydrogen fluoride);
In
tetrahydrofuran; ethanol; water; acetonitrile;
5: |Suzuki Coupling;
DOI:10.1016/j.bmc.2012.07.003