(4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

Base Information

Chemical Name:(4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol
CAS No.:173044-31-0
Molecular Formula:C₃₂H₄₆O₂Si
Molecular Weight:490.802
Hs Code.:

Synonyms:(4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

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Chemical Property of (4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

Chemical Property:

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Technology Process of (4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

There total 8 articles about (4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 173044-31-0
(4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / imidazole / dimethylformamide

2: 1.) n-BuLi, 2.) HMPA / 1.) THF, -78 deg C, 2.)THF, -94 deg C

3: HIO₄

4: NaBH₄

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; n-butyllithium; periodic acid; In N,N-dimethyl-formamide;
DOI:10.1021/ja9536779

Reference yield:

: (4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trienal

: 173044-31-0
(4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

Guidance literature:: With sodium tetrahydroborate; Yield given;
DOI:10.1021/ja9536779

Reference yield:

: 5233-99-8
10,11-epoxyfarnesol

: 173044-31-0
(4E,8E,11E)-13-(tert-Butyl-diphenyl-silanyloxy)-4,8,11-trimethyl-trideca-4,8,11-trien-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) CH₃SO₂Cl, 2.) LiCl

2: 1.) n-BuLi, 2.) HMPA / 1.) THF, -78 deg C, 2.)THF, -94 deg C

3: HIO₄

4: NaBH₄

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; n-butyllithium; methanesulfonyl chloride; periodic acid; lithium chloride;
DOI:10.1021/ja9536779