N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

Base Information

Chemical Name:N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine
CAS No.:113313-93-2
Molecular Formula:C₁₇H₂₂N₂
Molecular Weight:254.375
Hs Code.:

N<sup>2</sup>-benzyl-N<sup>1</sup>-methyl-1-phenyl-1,2-propanediamine

Synonyms:N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

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Technology Process of N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

There total 5 articles about N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 113313-92-1
1-benzyl-3,5-dimethyl-4-phenylimidazolidine

: 113313-93-2
N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

Guidance literature:: With hydrogenchloride; for 14h; Heating;
DOI:10.3987/R-1987-08-2129

Reference yield:

: 16735-25-4
α-Benzylamino-propiophenon-hydrochlorid

: 113313-93-2
N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

Guidance literature:: Multi-step reaction with 5 steps

1: 79 percent / H₂O / 1 h / Heating

2: 82 percent / H₂ / 10percent Pd/C / acetic acid / 6 h / 50 °C / 15001.2 Torr

3: 1.) NaH / 1.) DMF, from 0 deg C to 5 deg C, 2 h, 2.) DMF, RT

4: 88 percent / LiAlH₄ / tetrahydrofuran / 40 °C

5: 89 percent / 10percent aq. HCl / 14 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; water; acetic acid;
DOI:10.3987/R-1987-08-2129

Reference yield:

: 63235-71-2
1-benzyl-5-methyl-4-phenylimidazol-2-one

: 113313-93-2
N²-benzyl-N¹-methyl-1-phenyl-1,2-propanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / H₂ / 10percent Pd/C / acetic acid / 6 h / 50 °C / 15001.2 Torr

2: 1.) NaH / 1.) DMF, from 0 deg C to 5 deg C, 2 h, 2.) DMF, RT

3: 88 percent / LiAlH₄ / tetrahydrofuran / 40 °C

4: 89 percent / 10percent aq. HCl / 14 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium hydride; palladium on activated charcoal; In tetrahydrofuran; acetic acid;
DOI:10.3987/R-1987-08-2129