N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

Base Information

Chemical Name:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide
CAS No.:56784-91-9
Molecular Formula:C₂₆H₂₇N₃O₁₂
Molecular Weight:573.513
Hs Code.:

Synonyms:N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

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Chemical Property of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

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Technology Process of N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

There total 5 articles about N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1489282-54-3
C₂₈H₂₉N₃O₁₃

: 56784-91-9
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

Guidance literature:: With sodium cyanide; In methanol; at 25 ℃;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 116635-17-7
1-<(2,6-dimethyl-4-oxo-4H-<1>benzopyrano<3,4-d>oxazol-7-yl)oxy>-2-acetoxy-4-methoxy-5,5-dimethyl-3-tetrahydropyranyl 5-methyl-1H-pyrrole-2-carboxylate

: 56784-91-9
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 3 h / Reflux

2.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

2.2: 25 °C

3.1: sodium cyanide / methanol / 25 °C

With sodium cyanide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol;
DOI:10.1016/j.bmc.2013.06.042

Reference yield:

: 1476-53-5,6990-02-9,18656-99-0
sodium novobiocin

: 56784-91-9
N-(7-{[3-O-(aminocarbonyl)-6-deoxy-5-C-methyl-4-O-methyl-α-L-lyxohexopyranosyl]oxy}-4-hydroxy-8-methyl-2-oxo-2H-1-benzopyran-3-yl)-4-nitrobenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride / water

2.1: pyridine / 24 h / Reflux

3.1: ethanol / 3 h / Reflux

4.1: dicyclohexyl-carbodiimide; 4-pyrrolidin-1-ylpyridine / ethanol / 0.5 h / 25 °C

4.2: 25 °C

5.1: sodium cyanide / methanol / 25 °C

With pyridine; hydrogenchloride; sodium cyanide; 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In methanol; ethanol; water;
DOI:10.1016/j.bmc.2013.06.042