tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

Base Information

Chemical Name:tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate
CAS No.:1114592-27-6
Molecular Formula:C₁₉H₂₃ClN₄O₅S
Molecular Weight:454.934
Hs Code.:

Synonyms:tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

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Chemical Property of tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

Chemical Property:

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Technology Process of tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

There total 5 articles about tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1114592-21-0
4-{[(6-chloropyrimidin-4-yl)carbonyl]amino}-3-methylbenzenesulfonyl chloride

: 58620-93-2
tert-butyl 3-aminopropanoate hydrochloride

: 1114592-27-6
tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

Guidance literature:: With diisopropylamine; In tetrahydrofuran; at 20 ℃; for 18h;

Reference yield:

: 263270-52-6
6-chloropyrimidine-4-carbonyl chloride

: 1114592-27-6
tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.42 h

2: chlorosulfonic acid / dichloromethane / 0 - 20 °C

3: diisopropylamine / tetrahydrofuran / 18 h / 20 °C

With chlorosulfonic acid; diisopropylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 1114592-12-9
6-chloro-N-(2-methylphenyl)pyrimidine-4-carboxamide

: 1114592-27-6
tert-butyl 3-(4-(6-chloropyrimidine-4-carboxamido)-3-methylphenylsulfonamido)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / dichloromethane / 0 - 20 °C

2: diisopropylamine / tetrahydrofuran / 18 h / 20 °C

With chlorosulfonic acid; diisopropylamine; In tetrahydrofuran; dichloromethane;