C₂₈H₄₀O₈

Base Information

Chemical Name:C₂₈H₄₀O₈
CAS No.:1380327-86-5
Molecular Formula:C₂₈H₄₀O₈
Molecular Weight:504.621
Hs Code.:

C<sub>28</sub>H<sub>40</sub>O<sub>8</sub>

Synonyms:C₂₈H₄₀O₈

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Chemical Property of C₂₈H₄₀O₈

Chemical Property:

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Technology Process of C₂₈H₄₀O₈

There total 15 articles about C₂₈H₄₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: C₄₂H₅₂O₈

: 1380327-86-5
C₂₈H₄₀O₈

Guidance literature:: With 20 % Pd(OH)2/C; hydrogen; In ethyl acetate; at 20 ℃; for 0.333333h;
DOI:10.1021/jm300566h

Reference yield:

: 1380327-94-5
C₃₈H₅₆O₄S₂

: 1380327-86-5
C₂₈H₄₀O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: water; toluene-4-sulfonic acid / tetrahydrofuran; water; acetonitrile / 2 h / 20 °C

2.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C

3.1: camphor-10-sulfonic acid / dichloromethane; acetonitrile / 1 h / 20 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C

4.2: 1 h / 50 °C

5.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

6.1: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C

7.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 17 h / 20 °C / pH 7.2 / aq. phosphate buffer; Inert atmosphere

8.1: pyridine hydrogenfluoride / tetrahydrofuran / 6 h / 4 °C / aq. buffer

9.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

9.2: 20 °C

10.1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 0.33 h / 20 °C

With 1H-imidazole; potassium permanganate; sodium periodate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; 20 % Pd(OH)2/C; camphor-10-sulfonic acid; water; hydrogen; toluene-4-sulfonic acid; pyridine hydrogenfluoride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm300566h

Reference yield:

: C₃₅H₅₂O₄S₂

: 1380327-86-5
C₂₈H₄₀O₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / 20 °C / Molecular sieve

2.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

3.1: water; toluene-4-sulfonic acid / tetrahydrofuran; water; acetonitrile / 2 h / 20 °C

4.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C

5.2: 1 h / 50 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

7.1: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C

8.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 17 h / 20 °C / pH 7.2 / aq. phosphate buffer; Inert atmosphere

9.1: pyridine hydrogenfluoride / tetrahydrofuran / 6 h / 4 °C / aq. buffer

10.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 3 h / 20 °C

10.2: 20 °C

11.1: 20 % Pd(OH)2/C; hydrogen / ethyl acetate / 0.33 h / 20 °C

With 1H-imidazole; potassium permanganate; sodium periodate; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; 20 % Pd(OH)2/C; water; hydrogen; toluene-4-sulfonic acid; pyridine hydrogenfluoride; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; ethyl acetate; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm300566h