Technology Process of 2-Furancarboxylicacid,2,5-dihydro-5-methoxy-3-nitro-,methylester,(2S-cis)-(9CI)
There total 5 articles about 2-Furancarboxylicacid,2,5-dihydro-5-methoxy-3-nitro-,methylester,(2S-cis)-(9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonyl chloride; triethylamine;
In
chloroform;
for 1h;
DOI:10.1021/jo00364a015
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 95 percent / 60percent CH3COOH / 18 h / 35 - 40 °C
2: 71 percent / NaIO4, KHCO3, RuO2 / H2O; CCl4; acetonitrile / 2 h / 20 °C
3: 80 percent / Dowex-50 (H+ form) / methanol / 48 h / Heating
4: Et3N, CH3SO2Cl / CHCl3 / 1 h
With
ruthenium(IV) oxide; sodium periodate; Dowex-50 (H+ form); potassium hydrogencarbonate; acetic acid; methanesulfonyl chloride; triethylamine;
In
methanol; tetrachloromethane; chloroform; water; acetonitrile;
DOI:10.1021/jo00364a015
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 95 percent / 90percent H2O2, (CF3CO)2O, Na2HPO4, urea / acetonitrile / 0 - 5 °C
2: 95 percent / 60percent CH3COOH / 18 h / 35 - 40 °C
3: 71 percent / NaIO4, KHCO3, RuO2 / H2O; CCl4; acetonitrile / 2 h / 20 °C
4: 80 percent / Dowex-50 (H+ form) / methanol / 48 h / Heating
5: Et3N, CH3SO2Cl / CHCl3 / 1 h
With
ruthenium(IV) oxide; sodium periodate; disodium hydrogenphosphate; Dowex-50 (H+ form); dihydrogen peroxide; potassium hydrogencarbonate; acetic acid; methanesulfonyl chloride; triethylamine; urea; trifluoroacetic anhydride;
In
methanol; tetrachloromethane; chloroform; water; acetonitrile;
DOI:10.1021/jo00364a015
