1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

Base Information

Chemical Name:1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane
CAS No.:182156-62-3
Molecular Formula:C₃₀H₄₀N₄O₈
Molecular Weight:584.67
Hs Code.:

Synonyms:1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

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Chemical Property of 1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

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Technology Process of 1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

There total 3 articles about 1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 96-32-2
bromoacetic acid methyl ester

: 162148-45-0
1,4,7,10-tetraaza-cyclododecane-1,7-dicarboxylic acid dibenzyl ester

: 182156-62-3
1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

Guidance literature:: With potassium carbonate; In acetonitrile;
DOI:10.1016/0960-894X(96)00386-1

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 182156-62-3
1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ethanol; various solvent(s) / 24 h

2: 66 percent / K₂CO₃ / acetonitrile

With potassium carbonate; In ethanol; acetonitrile;
DOI:10.1016/0960-894X(96)00386-1

Reference yield:

: 294-90-6
1,4,7,10-tetraazacyclododecan

: 182156-62-3
1,7-Dicarboxymethyl-4,10-di(benzyloxycarbonyl)-1,4,7,10-tetrazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ethanol; various solvent(s) / 24 h

2: 66 percent / K₂CO₃ / acetonitrile

With potassium carbonate; In ethanol; acetonitrile;
DOI:10.1016/0960-894X(96)00386-1