methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate

Base Information

Chemical Name:methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate
CAS No.:1610831-07-6
Molecular Formula:C₁₉H₂₁ClO₅
Molecular Weight:364.826
Hs Code.:

Synonyms:methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate

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Technology Process of methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate

There total 2 articles about methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1610831-05-4
methyl 1-(2-bromo-4-methoxy-1,4-dioxobutyl)cyclohexanecarboxylate

: 104-88-1
4-chlorobenzaldehyde

: 1610831-07-6
methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate

Guidance literature:: With mercury dichloride; zinc; In ethyl acetate; benzene; for 2h; Heating;
DOI:10.1016/j.mencom.2014.04.019

Reference yield:

: 3196-23-4
methyl 1-bromocyclohexanecarboxylate

: 1610831-07-6
methyl 1-[2-(4-chlorophenyl)-5-oxotetrahydrofuran-3-carbonyl]cyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: zinc / ethyl acetate / 1 h / Reflux

2: bromine / acetic acid / 1 h / Heating

3: zinc; mercury dichloride / ethyl acetate; benzene / 2 h / Heating

With bromine; mercury dichloride; zinc; In acetic acid; ethyl acetate; benzene;
DOI:10.1016/j.mencom.2014.04.019