4-methylbenzenesulfenyl thiocyanate

Base Information

• Chemical Name: 4-methylbenzenesulfenyl thiocyanate
• CAS No.: 66067-70-7
• Molecular Formula: C₈H₇NS₂
• Molecular Weight: 181.282

Synonyms:4-methylbenzenesulfenyl thiocyanate

Chemical Property of 4-methylbenzenesulfenyl thiocyanate

Chemical Property:

Purity/Quality:

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Technology Process of 4-methylbenzenesulfenyl thiocyanate

There total 1 articles about 4-methylbenzenesulfenyl thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-methylbenzenesulfenyl chloride (933-00-6) + ammonium thiocyanate (1147550-11-5) → 4-methylbenzenesulfenyl thiocyanate (66067-70-7)

Guidance literature:

In tetrachloromethane; for 3h; Ambient temperature;

DOI:10.1021/jo00371a024

Reference yield: 82.0%

4-methylbenzenesulfenyl thiocyanate (66067-70-7) + 1-Methyleneamino-cyclohexanecarboxylic acid cyclohexylamide (134420-20-5) → 4-Cyclohexylamino-2-thioxo-1,3-diaza-spiro[4.5]dec-3-ene-1-carbothioic acid S-p-tolyl ester (134420-27-2)

Guidance literature:

In dichloromethane; 1) -30 degC, 2) to 20 degC;

Reference yield: 75.0%

4-methylbenzenesulfenyl thiocyanate (66067-70-7) + 1-Methyleneamino-cyclohexanecarboxylic acid phenylamide (134420-16-9) → 4-[(Z)-Phenylimino]-2-thioxo-1,3-diaza-spiro[4.5]decane-1-carbothioic acid S-p-tolyl ester (134420-30-7)

Guidance literature:

In dichloromethane; 1) -30 degC, 2) to 20 degC;

upstream raw materials:

p-methylbenzenesulfenyl chloride

ammonium thiocyanate

Downstream raw materials:

2-Methylsulfanyl-2-p-tolylsulfanyl-malonic acid dimethyl ester

4-Cyclohexylamino-2-thioxo-1,3-diaza-spiro[4.5]dec-3-ene-1-carbothioic acid S-p-tolyl ester

4-[(Z)-Phenylimino]-2-thioxo-1,3-diaza-spiro[4.5]decane-1-carbothioic acid S-p-tolyl ester

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