4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

Base Information

Chemical Name:4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate
CAS No.:252868-78-3
Molecular Formula:C₅₇H₉₆NO₁₂P
Molecular Weight:1018.36
Hs Code.:

Synonyms:4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

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Chemical Property of 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

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Technology Process of 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

There total 1 articles about 4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 183429-86-9
[(R)-2,3-bis{(1-oxohexadecyl)oxy}propyloxy](2-cyanoethoxy)(diisopropylamino)phosphane

: 156593-40-7
D-4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-myo-inositol

: 252868-78-3
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

Guidance literature:: [(R)-2,3-bis{(1-oxohexadecyl)oxy}propyloxy](2-cyanoethoxy)(diisopropylamino)phosphane; D-4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-myo-inositol; With 1H-tetrazole; In dichloromethane; at 20 ℃; for 6h;

With tert.-butylhydroperoxide; In dichloromethane;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 252868-78-3
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

: 6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero) phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / ethanol / 4 h / 20 °C / 3878.61 Torr

2: HCl / methanol / 3 h / 20 °C

3: Na; liq. NH₃ / methanol / -60 °C

With hydrogenchloride; ammonia; hydrogen; sodium; palladium on activated charcoal; In methanol; ethanol; 1: Hydrogenolysis / 2: Ring cleavage / 3: Substitution;
DOI:10.1016/S0040-4020(99)00793-0

Reference yield:

: 252868-78-3
4-O-benzyl-2,3-O-cyclohexylidene-6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

: 252868-84-1
6-deoxy-D-myo-inositol-1-(1,2-di-O-palmitoyl-sn-glycero)cyanoethyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / ethanol / 4 h / 20 °C / 3878.61 Torr

2: HCl / methanol / 3 h / 20 °C

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; ethanol; 1: Hydrogenolysis / 2: Ring cleavage;
DOI:10.1016/S0040-4020(99)00793-0