3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate

Base Information

Chemical Name:3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate
CAS No.:83831-29-2
Molecular Formula:CH₄O*C₁₃H₁₃N₅O₂S
Molecular Weight:335.387
Hs Code.:

Synonyms:3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate

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Technology Process of 3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate

There total 2 articles about 3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 75815-17-7
5-methyl-4-(3-aminophenyl)imidazole

: 79844-65-8
3,4-bis(methylthio)-1,2,5-thiadiazole 1-oxide

: 83831-29-2
3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate

Guidance literature:: In methanol; Ambient temperature;
DOI:10.1021/jm00356a005

Reference yield:

: 54887-79-5
5-methyl-4-(3-nitrophenyl)imidazole

: 83831-29-2
3-methoxy-4-<<3-(4-methyl-5-imidazolyl)phenyl>amino>-1,2,5-thiadiazole 1-oxide methanolate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / H₂, concd. HCl / 10percent Pd/C / ethanol / 4 h / 2585.7 Torr

2: 47 percent / methanol / Ambient temperature

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1021/jm00356a005