dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

Base Information

Chemical Name:dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]
CAS No.:180712-99-6
Molecular Formula:C₃₉H₃₉N₃O₁₁
Molecular Weight:725.752
Hs Code.:

Synonyms:dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

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Chemical Property of dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

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Technology Process of dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

There total 2 articles about dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 329-59-9
4-fluoro-3-nitro-benzoic acid methyl ester

: 86748-12-1
4,4'-(1-acetylpiperidine-4,4-diyl)-2,2',6,6'-tetramethylbis(phenol)

: 180712-99-6
dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 14h; Ambient temperature;
DOI:10.1002/hlca.19960790403

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 180712-99-6
dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / diethyl ether / ice cooling

2: 78 percent / K₂CO₃ / dimethylformamide / 14 h / Ambient temperature

With potassium carbonate; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19960790403

Reference yield: 99.0%

: 180712-99-6
dimethyl 4,4'-[(1-acetylpiperidin-4-ylidene)bis(2,6-dimethyl-4,1-phenyleneoxy)]bis[3-nitrobenzoate]

: 180713-00-2
C₃₇H₃₅N₃O₁₁

Guidance literature:: With potassium hydroxide; In tetrahydrofuran; methanol; water; for 4h; Ambient temperature;
DOI:10.1002/hlca.19960790403