C₅₁H₅₀O₁₆

Base Information

Chemical Name:C₅₁H₅₀O₁₆
CAS No.:1390643-92-1
Molecular Formula:C₅₁H₅₀O₁₆
Molecular Weight:918.948
Hs Code.:

C<sub>51</sub>H<sub>50</sub>O<sub>16</sub>

Synonyms:C₅₁H₅₀O₁₆

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Chemical Property of C₅₁H₅₀O₁₆

Chemical Property:

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Technology Process of C₅₁H₅₀O₁₆

There total 15 articles about C₅₁H₅₀O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 869996-05-4
O-(methyl 2,3,4-tri-O-acetyl-D-glucuronopyranosyl)-N-phenyl-2,2,2-trifluoroacetimidate

: 1390643-90-9
(2R,3R)-5,7,3'-tri-O-benzyl-3-acetylepicatechin

: 1390643-92-1
C₅₁H₅₀O₁₆

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at 0 - 20 ℃; for 17h;
DOI:10.1021/ol3016463

Reference yield:

: 889471-78-7
(E)-2-(benzyloxy)-4-(3-hydroxyprop-1-en-1-yl)phenol

: 1390643-92-1
C₅₁H₅₀O₁₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: Montmorillonite K-10 clay / dichloromethane / 0.25 h / 20 °C / Inert atmosphere

1.2: 13.5 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

3.1: AD-mix-α; methanesulfonamide / dichloromethane; water; tert-butyl alcohol / 72 h / 0 - 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

5.1: pyridinium p-toluenesulfonate / 1,2-dichloro-ethane / 5.3 h / 20 - 55 °C / Inert atmosphere

6.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 48 h / 20 °C / Inert atmosphere

7.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C / Inert atmosphere

8.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C / Inert atmosphere

9.1: L-Selectride / tetrahydrofuran / 8 h / -78 °C / Inert atmosphere

10.1: pyridine; dmap / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

12.1: boron trifluoride diethyl etherate / dichloromethane / 17 h / 0 - 20 °C

With pyridine; dmap; methanesulfonamide; AD-mix-α; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; L-Selectride; diisobutylaluminium hydride; Dess-Martin periodane; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; toluene; tert-butyl alcohol; 1.1: Friedel Crafts alkylation / 1.2: Friedel Crafts alkylation;
DOI:10.1021/ol3016463

Reference yield:

: 1390643-82-9
(2R)-4'-(tert-butyldimethylsilyloxy)-5,7,3'-tribenzyloxyflavan-3-one

: 1390643-92-1
C₅₁H₅₀O₁₆

Guidance literature:: Multi-step reaction with 4 steps

1: L-Selectride / tetrahydrofuran / 8 h / -78 °C / Inert atmosphere

2: pyridine; dmap / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

4: boron trifluoride diethyl etherate / dichloromethane / 17 h / 0 - 20 °C

With pyridine; dmap; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; L-Selectride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol3016463