4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide

Base Information

• Chemical Name: 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide
• CAS No.: 1064780-96-6
• Molecular Formula: C₁₈H₂₃NO₃SSi
• Molecular Weight: 361.537

Synonyms:4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide

Chemical Property of 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide

Chemical Property:

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Technology Process of 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide

There total 1 articles about 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

phenyl(trimethylsilylethynyl)iodonium triflate (133816-00-9) + 4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide (167847-61-2) → 4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide (1064780-96-6)

Guidance literature:

4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide; With n-butyllithium; In hexane; toluene; at 0 ℃; for 1h;

phenyl(trimethylsilylethynyl)iodonium triflate; In hexane; toluene; at 20 ℃; for 16h;

DOI:10.1002/chem.200800210

Reference yield: 99.0%

4-methyl-N-[(5-methylfuran-2-yl)methyl]-N-[(trimethylsilyl)ethynyl]benzenesulfonamide (1064780-96-6) → N-ethynyl-4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide (1064781-00-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 0.0833333h;

DOI:10.1002/chem.200800210

upstream raw materials:

phenyl(trimethylsilylethynyl)iodonium triflate

4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide

Downstream raw materials:

N-ethynyl-4-methyl-N-[(5-methylfuran-2-yl)methyl]benzenesulfonamide

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