N-methyl-N--2-phenylglycine ethyl ester

Base Information

Chemical Name:N-methyl-N--2-phenylglycine ethyl ester
CAS No.:81278-22-0
Molecular Formula:C₂₃H₂₇NO₄
Molecular Weight:381.472
Hs Code.:

N-methyl-N-<p-methoxy-o-(3-butenyl)benzoyl>-2-phenylglycine ethyl ester

Synonyms:N-methyl-N--2-phenylglycine ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N--2-phenylglycine ethyl ester

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Technology Process of N-methyl-N--2-phenylglycine ethyl ester

There total 2 articles about N-methyl-N--2-phenylglycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81278-33-3
2--4,4-dimethyl-Δ²-oxazoline

: 81278-22-0
N-methyl-N--2-phenylglycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) methyl iodide, 2.) aq. sodium hydroxide / 1.) reflux, 20 h, 2.) THF, reflux, 26 h

2: 1.) oxalyl chloride, N,N-dimethylformamide, 2.) triethylamine / 1.) ether, 5 deg C, 19 h, 2.) benzene, 25 deg C, 8 h

With sodium hydroxide; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; methyl iodide;
DOI:10.1021/jo00133a041

Reference yield:

: 81278-31-1
N-methyl-2-phenylglycine ethyl ester

: 81278-32-2
p-methoxy-o-(3-butenyl)benzoic acid

: 81278-22-0
N-methyl-N--2-phenylglycine ethyl ester

Guidance literature:: With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; Yield given. Multistep reaction; 1.) ether, 5 deg C, 19 h, 2.) benzene, 25 deg C, 8 h;
DOI:10.1021/jo00133a041