1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

Base Information

Chemical Name:1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile
CAS No.:171858-64-3
Molecular Formula:C₂₇H₂₆N₂
Molecular Weight:378.517
Hs Code.:

Synonyms:1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

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Chemical Property of 1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

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Technology Process of 1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

There total 4 articles about 1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-Benzyl-4-(2-cyano-2,2-diphenyl-ethyl)-pyridinium; bromide

: 171858-64-3
1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 0 ℃; for 0.5h; Yield given;
DOI:10.1021/jo00123a014

Reference yield:

: 86-29-3
Diphenylacetonitrile

: 171858-64-3
1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 50percent aq. NaOH, hexadecyltributylphosphonium bromide / toluene / 4 h

2: 92 percent / propan-2-ol / 0.17 h / Heating

3: NaBH₄ / ethanol / 0.5 h / 0 °C

With sodium hydroxide; sodium tetrahydroborate; cetyltributylphosphonium bromide; In ethanol; isopropyl alcohol; toluene;
DOI:10.1021/jo00123a014

Reference yield:

: 1822-51-1
4-picolylchloride hydrochloride

: 171858-64-3
1-(Phenylmethyl)-α,α-diphenyl-1,2,5,6-tetrahydro-4-pyridinepropanenitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / 50percent aq. NaOH, hexadecyltributylphosphonium bromide / toluene / 4 h

2: 92 percent / propan-2-ol / 0.17 h / Heating

3: NaBH₄ / ethanol / 0.5 h / 0 °C

With sodium hydroxide; sodium tetrahydroborate; cetyltributylphosphonium bromide; In ethanol; isopropyl alcohol; toluene;
DOI:10.1021/jo00123a014