(1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester

Base Information

• Chemical Name: (1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester
• CAS No.: 365240-72-8
• Molecular Formula: C₁₃H₂₁BrO₃
• Molecular Weight: 305.212

Synonyms:(1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester

Chemical Property of (1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester

Chemical Property:

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Technology Process of (1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester

There total 1 articles about (1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-bromo-2-methyl-3-oxodec-7(Z)-enoate (135482-44-9) → (1S,2R)-2-((R)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester + (1S,2R)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester + (1R,2S)-2-((R)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester + (1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester (365240-72-8)

Guidance literature:

ethyl 2-bromo-2-methyl-3-oxodec-7(Z)-enoate; With magnesium(II) perchlorate; 4 A molecular sieve; 2,2'-isopropylidenebis[(4S)-4-tert-butyl-2-oxazoline]; In toluene; at 20 ℃; for 0.5h;

With triethyl borane; oxygen; In hexane; toluene; at -78 ℃; Further stages.;

DOI:10.1021/ja016383y

Reference yield: 78.0%

(1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester (365240-72-8) + (2,4-dinitro-phenyl)-hydrazine (119-26-6) → (1R,2S)-2-((S)-1-Bromo-propyl)-6-[(2,4-dinitro-phenyl)-hydrazono]-1-methyl-cyclohexanecarboxylic acid ethyl ester

Guidance literature:

In ethanol;

DOI:10.1021/ja016383y

Reference yield:

(1R,2S)-2-((S)-1-Bromo-propyl)-1-methyl-6-oxo-cyclohexanecarboxylic acid ethyl ester (365240-72-8) → (1R,6S)-1-Methyl-2-oxo-6-propyl-cyclohexanecarboxylic acid ethyl ester

Guidance literature:

With triethyl borane; oxygen; tri-n-butyl-tin hydride; In hexane; benzene; at 20 ℃;

DOI:10.1021/ja016383y

upstream raw materials:

ethyl 2-bromo-2-methyl-3-oxodec-7(Z)-enoate

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