N-phenyl-α,α-dichloroacetohydroxamic acid

Base Information

Chemical Name:N-phenyl-α,α-dichloroacetohydroxamic acid
CAS No.:34282-44-5
Molecular Formula:C₈H₇Cl₂NO₂
Molecular Weight:220.055
Hs Code.:

Synonyms:N-phenyl-α,α-dichloroacetohydroxamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-α,α-dichloroacetohydroxamic acid

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Technology Process of N-phenyl-α,α-dichloroacetohydroxamic acid

There total 3 articles about N-phenyl-α,α-dichloroacetohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 79-36-7
dichloroacethyl chloride

: 100-65-2
N-Phenylhydroxylamine

: 34282-44-5
N-phenyl-α,α-dichloroacetohydroxamic acid

Guidance literature:: With sodium hydrogencarbonate; In di-isopropyl ether; at 0 - 5 ℃; for 0.5h;
DOI:10.1021/jo00368a029

Reference yield:

: 98-95-3,26969-40-4
nitrobenzene

: 34282-44-5
N-phenyl-α,α-dichloroacetohydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: rhodium on carbon; hydrazine hydrate / tetrahydrofuran / 0 - 23 °C

2: sodium hydrogencarbonate / diethyl ether / 12 h / 0 - 23 °C

With rhodium on carbon; sodium hydrogencarbonate; hydrazine hydrate; In tetrahydrofuran; diethyl ether;
DOI:10.1002/anie.202100801