15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Base Information

Chemical Name:15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid
CAS No.:443770-20-5
Molecular Formula:C₅₆H₇₃N₃O₃
Molecular Weight:836.214
Hs Code.:

Synonyms:15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Suppliers and Price of 15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

There total 3 articles about 15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 443770-19-2
15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid 2-oxo-2-phenyl-ethyl ester

: 443770-20-5
15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Guidance literature:: With 1H-imidazole; sodium hydride; thiophenol; In N,N-dimethyl-formamide; at 25 ℃;
DOI:10.1016/S0040-4039(02)00338-6

Reference yield:

: 505-54-4
thapsic acid

: 443770-20-5
15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / iPr₂NEt / dimethylformamide / 24 h / 25 °C

2: 60 percent / bromotripyrrolidinophosphonium hexafluorophosphate; iPr₂NEt / dimethylformamide / 3.5 h / 0 - 25 °C

3: 60 percent / PhSH; NaH; imidazole / dimethylformamide / 25 °C

With 1H-imidazole; sodium hydride; thiophenol; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)00338-6

Reference yield:

: 443770-14-7
hexadecanedioic acid mono-(2-oxo-2-phenyl-ethyl) ester

: 443770-20-5
15-{(4-dibenzylamino-butyl)-[3-(trityl-amino)-propyl]-carbamoyl}-pentadecanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / bromotripyrrolidinophosphonium hexafluorophosphate; iPr₂NEt / dimethylformamide / 3.5 h / 0 - 25 °C

2: 60 percent / PhSH; NaH; imidazole / dimethylformamide / 25 °C

With 1H-imidazole; sodium hydride; thiophenol; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(02)00338-6