4-amino-3-(N-methylacetamido)toluene

Base Information

Chemical Name:4-amino-3-(N-methylacetamido)toluene
CAS No.:155221-55-9
Molecular Formula:C₁₀H₁₄N₂O
Molecular Weight:178.234
Hs Code.:

Synonyms:4-amino-3-(N-methylacetamido)toluene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-amino-3-(N-methylacetamido)toluene

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Technology Process of 4-amino-3-(N-methylacetamido)toluene

There total 8 articles about 4-amino-3-(N-methylacetamido)toluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 155221-54-8
3-(N-methylacetamido)-4-nitrotoluene

: 155221-55-9
4-amino-3-(N-methylacetamido)toluene

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4h; under 2585.7 Torr;
DOI:10.1021/jm00027a010

Reference yield:

: 578-46-1
5-methyl-2-nitroaniline

: 155221-55-9
4-amino-3-(N-methylacetamido)toluene

Guidance literature:: Multi-step reaction with 4 steps

1: trifluoroacetic acid / 1 h / Ambient temperature

2: KOH / acetone / 8 h / Heating

3: 81 percent / pyridine / CH₂Cl₂ / 8 h / Heating

4: 96 percent / H₂ / 5percent Pd on charcoal / methanol / 4 h / 2585.7 Torr

With pyridine; potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetone; trifluoroacetic acid;
DOI:10.1021/jm00027a010

Reference yield:

: 155221-62-8
5-methyl-2-nitrotrifluoroacetanilide

: 155221-55-9
4-amino-3-(N-methylacetamido)toluene

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / acetone / 8 h / Heating

2: 81 percent / pyridine / CH₂Cl₂ / 8 h / Heating

3: 96 percent / H₂ / 5percent Pd on charcoal / methanol / 4 h / 2585.7 Torr

With pyridine; potassium hydroxide; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetone;
DOI:10.1021/jm00027a010