5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

Base Information

Chemical Name:5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide
CAS No.:202823-10-7
Molecular Formula:C₁₅H₁₂ClF₃N₂O₂
Molecular Weight:344.721
Hs Code.:

5-chloro-2-methoxy-benzoic acid <i>N</i>'-(4-trifluoromethyl-phenyl)-hydrazide

Synonyms:5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

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Chemical Property of 5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

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Technology Process of 5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

There total 1 articles about 5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3438-16-2
5-chloro-2-methoxybenzoic acid

: 368-90-1
4-(trifluoromethyl)phenylhydrazine

: 202823-10-7
5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

Guidance literature:: 5-chloro-2-methoxybenzoic acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 20 ℃; for 0.5h;

4-(trifluoromethyl)phenylhydrazine; In tetrahydrofuran; for 8h;
DOI:10.1021/jm061006n

Reference yield:

: 202823-10-7
5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

: 530-62-1
1,1'-carbonyldiimidazole

: 202823-13-0
5-(5-chloro-2-methoxy-phenyl)-3-(4-trifluoromethyl-phenyl)-3H-[1,3,4]oxadiazol-2-one

Guidance literature:: With triethylamine; In tetrahydrofuran; at 24 ℃; for 18h;
DOI:10.1021/jm061006n

Reference yield:

: 202823-10-7
5-chloro-2-methoxy-benzoic acid N'-(4-trifluoromethyl-phenyl)-hydrazide

: 5-(5-Chloro-2-hydroxyphenyl)-3-[4-(trifluoromethyl)phenyl]-1,3,4-oxadiazol-2-(3H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 18 h / 24 °C

2: BBr₃ / CH₂Cl₂ / 18 h / 24 °C

With boron tribromide; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm061006n