N-tert-butyl(phenylthio)formimidoyl isothiocyanate

Base Information

• Chemical Name: N-tert-butyl(phenylthio)formimidoyl isothiocyanate
• CAS No.: 104157-42-8
• Molecular Formula: C₁₂H₁₄N₂S₂
• Molecular Weight: 250.389

Synonyms:N-tert-butyl(phenylthio)formimidoyl isothiocyanate

Chemical Property of N-tert-butyl(phenylthio)formimidoyl isothiocyanate

Chemical Property:

Purity/Quality:

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Technology Process of N-tert-butyl(phenylthio)formimidoyl isothiocyanate

There total 2 articles about N-tert-butyl(phenylthio)formimidoyl isothiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butylisonitrile (119072-55-8,7188-38-7) + benzenesulfenyl thiocyanate (3153-52-4) → N-tert-butyl(phenylthio)formimidoyl isothiocyanate (104157-42-8)

Guidance literature:

In tetrachloromethane; at 0 ℃;

DOI:10.1021/jo00371a024

Reference yield:

ammonium thiocyanate (1147550-11-5) + C11H14ClNS (90496-27-8) → N-tert-butyl(phenylthio)formimidoyl isothiocyanate (104157-42-8)

Guidance literature:

In tetrachloromethane; for 3h; Ambient temperature;

DOI:10.1021/jo00371a024

Reference yield: 60.0%

benzenesulfenyl thiocyanate (3153-52-4) + N-tert-butyl(phenylthio)formimidoyl isothiocyanate (104157-42-8) → 1-tert-butyl-2,5-bis(phenylthio)-1,3,4,6,6a-triazadithia(6aSIV)pentalene (104157-57-5)

Guidance literature:

In tetrachloromethane; at 20 ℃; for 0.25h;

DOI:10.1021/jo00371a024

upstream raw materials:

tert-butylisonitrile

benzenesulfenyl thiocyanate

ammonium thiocyanate

C₁₁H₁₄ClNS

Downstream raw materials:

1-tert-butyl-2,5-bis(phenylthio)-1,3,4,6,6a-triazadithia(6aS^IV)pentalene

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