(1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.0^3,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester

Base Information

• Chemical Name: (1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.0^3,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester
• CAS No.: 249581-28-0
• Molecular Formula: C₂₇H₂₉NO₆
• Molecular Weight: 463.53

Synonyms:(1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.0^3,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester

Chemical Property of (1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.0^3,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester

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Technology Process of (1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.0^3,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester

There total 1 articles about (1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.0^3,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

(1R,3R,5R,7S)-3-Benzoyl-8-oxo-6-aza-bicyclo[3.2.1]octane-6,7-dicarboxylic acid 6-benzyl ester 7-tert-butyl ester (249581-24-6) → (1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.03,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester (249581-28-0)

Guidance literature:

In dichloromethane; at 25 ℃; Irradiation;

DOI:10.1055/s-1999-2843

Reference yield: 76.0%

(1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.03,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester (249581-28-0) → (1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.03,7]nonane-3-carboxylic acid tert-butyl ester

Guidance literature:

With cyclohexene; 10% palladium on active carbon; In methanol; for 1.5h; Heating;

DOI:10.1055/s-1999-2843

Reference yield:

(1R,3R,4R,5R,7R)-4-Hydroxy-8-oxo-4-phenyl-2-aza-tricyclo[3.3.1.03,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester (249581-28-0) → (1R,3R,4R,5R,7R,8R)-4,8-Dihydroxy-4-phenyl-2-aza-tricyclo[3.3.1.03,7]nonane-2,3-dicarboxylic acid 2-benzyl ester 3-tert-butyl ester

Guidance literature:

With sodium tetrahydroborate;

DOI:10.1055/s-1999-2843

upstream raw materials:

(1R,3R,5R,7S)-3-Benzoyl-8-oxo-6-aza-bicyclo[3.2.1]octane-6,7-dicarboxylic acid 6-benzyl ester 7-tert-butyl ester

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