C₃₈H₄₅N₃O₁₁

Base Information

Chemical Name:C₃₈H₄₅N₃O₁₁
CAS No.:1381853-64-0
Molecular Formula:C₃₈H₄₅N₃O₁₁
Molecular Weight:719.789
Hs Code.:

C<sub>38</sub>H<sub>45</sub>N<sub>3</sub>O<sub>11</sub>

Synonyms:C₃₈H₄₅N₃O₁₁

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Chemical Property of C₃₈H₄₅N₃O₁₁

Chemical Property:

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Technology Process of C₃₈H₄₅N₃O₁₁

There total 14 articles about C₃₈H₄₅N₃O₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1445-45-0
Trimethyl orthoacetate

: 1381853-62-8
C₃₅H₄₁N₃O₁₀

: 1381853-64-0
C₃₈H₄₅N₃O₁₁

Guidance literature:: With 10-camphorsufonic acid; In acetonitrile; at 20 ℃; for 0.333333h;

Reference yield:

: 73-34-7
L-rhamnose

: 1381853-64-0
C₃₈H₄₅N₃O₁₁

Guidance literature:: Multi-step reaction with 17 steps

1.1: iodine / 12 h / 20 °C

2.1: ammonia / tetrahydrofuran / 14 h / 0 - 20 °C

3.1: potassium carbonate / dichloromethane / 0.67 h / 20 °C

4.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.67 h / 20 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide / 4 h / 65 °C / Inert atmosphere

6.1: acetyl chloride; methanol / 12 h / 0 - 20 °C

7.1: 12 h / 20 °C

8.1: sodium hydride / 1-methyl-pyrrolidin-2-one; tetrahydrofuran; mineral oil / 0.08 h / 0 °C

8.2: 12.5 h / 0 - 20 °C

9.1: trifluoroacetic acid; water / tetrahydrofuran / 12 h / 20 °C

10.1: 10-camphorsufonic acid / acetonitrile / 0.33 h / 20 °C

11.1: water / acetonitrile / 0.33 h / 20 °C

12.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1.17 h / 20 °C / Inert atmosphere

13.1: sodium methylate; methanol / tetrahydrofuran / 2 h / 40 °C

14.1: Amberlyst_.(R). 15 hydrogen form resin / 0.5 h / 20 °C

15.1: pyridine / 1.17 h / 20 °C

16.1: water; acetic acid / 12 h / 20 °C

17.1: 10-camphorsufonic acid / acetonitrile / 0.33 h / 20 °C

With pyridine; methanol; sodium azide; trimethylsilyl trifluoromethanesulfonate; 10-camphorsufonic acid; ammonia; water; iodine; sodium methylate; sodium hydride; potassium carbonate; acetic acid; acetyl chloride; trifluoroacetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1381853-32-2
C₁₁H₁₉N₃O₅

: 1381853-64-0
C₃₈H₄₅N₃O₁₁

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one; tetrahydrofuran; mineral oil / 0.08 h / 0 °C

1.2: 12.5 h / 0 - 20 °C

2.1: trifluoroacetic acid; water / tetrahydrofuran / 12 h / 20 °C

3.1: 10-camphorsufonic acid / acetonitrile / 0.33 h / 20 °C

4.1: water / acetonitrile / 0.33 h / 20 °C

5.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1.17 h / 20 °C / Inert atmosphere

6.1: sodium methylate; methanol / tetrahydrofuran / 2 h / 40 °C

7.1: Amberlyst_.(R). 15 hydrogen form resin / 0.5 h / 20 °C

8.1: pyridine / 1.17 h / 20 °C

9.1: water; acetic acid / 12 h / 20 °C

10.1: 10-camphorsufonic acid / acetonitrile / 0.33 h / 20 °C

With pyridine; methanol; trimethylsilyl trifluoromethanesulfonate; 10-camphorsufonic acid; water; sodium methylate; sodium hydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dichloromethane; acetonitrile; mineral oil;