C₁₅H₁₃ClN₂OS

Base Information

Chemical Name:C₁₅H₁₃ClN₂OS
CAS No.:1420626-73-8
Molecular Formula:C₁₅H₁₃ClN₂OS
Molecular Weight:304.8
Hs Code.:

C<sub>15</sub>H<sub>13</sub>ClN<sub>2</sub>OS

Synonyms:C₁₅H₁₃ClN₂OS

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Chemical Property of C₁₅H₁₃ClN₂OS

Chemical Property:

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Technology Process of C₁₅H₁₃ClN₂OS

There total 7 articles about C₁₅H₁₃ClN₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1420830-33-6
4-chloro-2-methylthiophene-3-carboxylic acid

: 146553-06-2,87694-49-3
tert-butyl {(S)-1-[methoxy(methyl)amino]-1-oxopropan-2-yl}carbamate

: 1420626-73-8
C₁₅H₁₃ClN₂OS

Guidance literature:: 4-chloro-2-methylthiophene-3-carboxylic acid; With n-butyllithium; In tetrahydrofuran; hexane; at -60 - -50 ℃; for 0.5h; Inert atmosphere;

tert-butyl {(S)-1-[methoxy(methyl)amino]-1-oxopropan-2-yl}carbamate; With isopropylmagnesium chloride; In tetrahydrofuran; at -60 - 20 ℃; for 3h; Inert atmosphere;

With hydrogenchloride; In water; at 0 ℃; pH=5 - 6; Reflux;

Reference yield:

: 2158-82-9
4-hydroxy-2-methyl-thiophene-3-carboxylic acid ethyl ester

: 1420626-73-8
C₁₅H₁₃ClN₂OS

Guidance literature:: Multi-step reaction with 6 steps

1.1: trichlorophosphate / N,N-dimethyl-formamide / 1.5 h / 20 - 80 °C / Inert atmosphere

2.1: Oxone / N,N-dimethyl-formamide / 20 °C

2.2: 0.5 h

3.1: acetic acid; mercury(II) oxide / 1 h / Reflux

3.2: 1 h / Reflux

4.1: water; sodium hydroxide / ethanol / 1 h / Reflux

5.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 - 20 °C

6.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -60 - -50 °C / Inert atmosphere

6.2: 3 h / -60 - 20 °C / Inert atmosphere

6.3: 0 °C / pH 5 - 6 / Reflux

With Oxone; n-butyllithium; oxalyl dichloride; water; acetic acid; N,N-dimethyl-formamide; mercury(II) oxide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 37479-76-8
ethyl 4-chloro-5-formyl-2-methylthiophene-3-carboxylate

: 1420626-73-8
C₁₅H₁₃ClN₂OS

Guidance literature:: Multi-step reaction with 5 steps

1.1: Oxone / N,N-dimethyl-formamide / 20 °C

1.2: 0.5 h

2.1: acetic acid; mercury(II) oxide / 1 h / Reflux

2.2: 1 h / Reflux

3.1: water; sodium hydroxide / ethanol / 1 h / Reflux

4.1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 0 - 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -60 - -50 °C / Inert atmosphere

5.2: 3 h / -60 - 20 °C / Inert atmosphere

5.3: 0 °C / pH 5 - 6 / Reflux

With Oxone; n-butyllithium; oxalyl dichloride; water; acetic acid; N,N-dimethyl-formamide; mercury(II) oxide; sodium hydroxide; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;