bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]

Base Information

Chemical Name:bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]
CAS No.:869337-79-1
Molecular Formula:C₃₈H₄₀N₂O₁₂
Molecular Weight:716.742
Hs Code.:

Synonyms:bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]

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Technology Process of bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]

There total 2 articles about bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 869337-75-7
benzyl 3,5-dimethyl-4-(ethanoic acid)pyrrole-2-carboxylate

: 608-68-4
dimethyl L-tartrate

: 869337-79-1
bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol052044o

Reference yield:

: 31837-62-4
benzyl 4-<(methoxycarbonyl)methyl>-3,5-dimethylpyrrole-2-carboxylate

: 869337-79-1
bis[benzyl 4,4'-[dimethyl-(R,R)-tartrylethanoate-3,5-dimethyl]-1H-pyrrole-2-carboxylate]

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 24 h / 20 °C

2: 82 percent / DCC; DMAP / tetrahydrofuran / 20 °C

With dmap; lithium hydroxide; dicyclohexyl-carbodiimide; In tetrahydrofuran; water;
DOI:10.1021/ol052044o