(2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

Base Information

Chemical Name:(2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine
CAS No.:872360-66-2
Molecular Formula:C₃₄H₃₇NO₄
Molecular Weight:523.672
Hs Code.:

Synonyms:(2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

There total 7 articles about (2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1454797-15-9
(2S,3R,4R,5S)-1-benzyl-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-5-(trityloxymethyl)-pyrrolidine

: 872360-66-2
(2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo401613v

Reference yield:

: (2R,3R,4R,5S)-1-Benzyl-3,4-bis-benzyloxy-5-benzyloxymethyl-pyrrolidine-2-carbaldehyde

: 872360-66-2
(2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2005.07.001

Reference yield:

: 151507-95-8
(2S,3R,4R,5S)-N-benzyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-2-vinyl-pyrrolidine

: 872360-66-2
(2S,3R,4R,5S)-N-benzyl-2-hydroxymethyl-3,4-dibenzyloxy-5-[(benzyloxy)methyl]-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: O₃; H₂SO₄ / CH₂Cl₂ / 0.42 h / -50 °C

1.2: Me₂S / CH₂Cl₂

2.1: 1.006 g / NaBH₄ / ethanol / 1 h / 20 °C

With sodium tetrahydroborate; sulfuric acid; ozone; In ethanol; dichloromethane;
DOI:10.1016/j.ejmech.2005.07.001