4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

Base Information

Chemical Name:4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester
CAS No.:439675-16-8
Molecular Formula:C₁₃H₂₀OSe₂Si
Molecular Weight:378.307
Hs Code.:

Synonyms:4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

Suppliers and Price of 4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

There total 3 articles about 4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 52630-10-1
4-methoxyselenobenzoic acid O-methyl ester

: 439675-12-4
bis[2-(trimethylsilyl)ethyl]-diselenide

: 439675-16-8
4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

Guidance literature:: bis[2-(trimethylsilyl)ethyl]-diselenide; With diisobutylaluminium hydride; In toluene; at 30 ℃; for 0.166667h;

4-methoxyselenobenzoic acid O-methyl ester; In toluene; at 30 ℃; for 5h; Further stages.;
DOI:10.1021/ja026110i

Reference yield:

: 18156-67-7
(2-bromoethyl)trimethylsilane

: 439675-16-8
4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1.074 g / Li₂Se₂ / CH₂Cl₂; tetrahydrofuran / 0 - 30 °C

2.1: DIBAL-H / toluene / 0.17 h / 30 °C

2.2: 27 percent / toluene / 5 h / 30 °C

With dilithium diselenide; diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja026110i

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 439675-16-8
4-methoxydiselenobenzoic acid Se-2-(trimethylsilyl)ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: CBr₄; PPh₃ / CH₂Cl₂ / 0.37 h / 0 °C

2.1: 1.074 g / Li₂Se₂ / CH₂Cl₂; tetrahydrofuran / 0 - 30 °C

3.1: DIBAL-H / toluene / 0.17 h / 30 °C

3.2: 27 percent / toluene / 5 h / 30 °C

With dilithium diselenide; carbon tetrabromide; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1021/ja026110i