2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline

Base Information

Chemical Name:2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline
CAS No.:1215022-34-6
Molecular Formula:C₄₂H₅₀N₄O₂Si₂
Molecular Weight:699.056
Hs Code.:

Synonyms:2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline

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Chemical Property of 2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline

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Technology Process of 2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline

There total 1 articles about 2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1215022-29-9
(S)-2-((tert-butyldimethylsilyloxy)(phenyl)methyl)-4-chloroquinazoline

: C₂₁H₂₆N₂OSi

: 1215022-24-4
(S)-2-((tert-butyldimethylsilyloxy)(phenyl)methyl)quinazolin-4(3H)-one

: 1215022-34-6
2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline

Guidance literature:: With triphenylphosphine; nickel dichloride; zinc; In N,N-dimethyl-formamide; at 50 ℃; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.12.002

Reference yield: 48.0%

: 1215022-34-6
2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline

: 1215022-39-1
(1S,1'S)-1,1'-(4,4'-biquinazoline-2,2'-diyl)-bis-(phenylmethanol)

Guidance literature:: 2,2'-bis-((S)-(tert-butyldimethylsilyloxy)(phenyl)methyl)-4,4'-biquinazoline; With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

With water; ammonium chloride; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2009.12.002