Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

Base Information

Chemical Name:Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester
CAS No.:132585-93-4
Molecular Formula:C₂₂H₃₀O₇S
Molecular Weight:438.542
Hs Code.:

Synonyms:Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

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Chemical Property of Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

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Technology Process of Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

There total 1 articles about Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 15539-61-4
Acetic acid (E)-3-phenylsulfanyl-allyl ester

: 23568-31-2
2,3:4,5-di-O-isopropylidene-L-arabinose

: 132585-93-4
Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 7h;
DOI:10.1016/S0040-4039(00)74336-X

Reference yield:

: 132585-93-4
Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

: 134615-02-4
Acetic acid (2R,3R,4R,5R)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-hydroxy-2-phenylsulfanyl-tetrahydro-furan-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: aq. CF₃COOH

2: NaIO₄ / H₂O

3: NaBH₄

4: 84 percent / Et₃N / DMAP

With sodium tetrahydroborate; sodium periodate; triethylamine; trifluoroacetic acid; dmap; In water;
DOI:10.1016/S0040-4039(00)74336-X

Reference yield:

: 132585-93-4
Acetic acid (4S,4aS,6R,7R,7aR)-4-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,2-d][1,3]dioxin-7-ylmethyl ester

: Acetic acid (2R,3S,4S,5S)-4-azido-5-hydroxymethyl-2-phenylsulfanyl-tetrahydro-furan-3-ylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: aq. CF₃COOH

2: NaIO₄ / H₂O

3: NaBH₄

4: 84 percent / Et₃N / DMAP

5: 1) pyridine, 2) sodium azide / 2) DMF, 100 deg C

With pyridine; sodium tetrahydroborate; sodium periodate; sodium azide; triethylamine; trifluoroacetic acid; dmap; In water;
DOI:10.1016/S0040-4039(00)74336-X