Technology Process of C36H25BrO4
There total 8 articles about C36H25BrO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) hydrazine hydrate, 2.) KOH / 1.) triethylene glycol, 110 deg C, 60 min, 2.) 140 deg C, 2 h
2: 20 percent / benzene; acetic acid / 5 h / 80 °C
3: 99 percent / conc. HCl / acetic acid / 1 h / Heating
4: 66 percent / iodine / tetrahydrofuran; benzene / 3 h / 80 °C
5: N-bromosuccinimid (NBS), 2,2'-azobis(isobutyronitrile) / CCl4 / 0.67 h / Heating; Irradiation
With
potassium hydroxide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine; hydrazine hydrate;
hydrogenchloride;
In
tetrahydrofuran; tetrachloromethane; acetic acid; benzene;
DOI:10.1021/jo00342a041
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 65 percent / n-pentanol, sodium / 4 h / Heating
2: 61 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / benzene / 96 h / Ambient temperature
3: 20 percent / benzene; acetic acid / 5 h / 80 °C
4: 99 percent / conc. HCl / acetic acid / 1 h / Heating
5: 66 percent / iodine / tetrahydrofuran; benzene / 3 h / 80 °C
6: N-bromosuccinimid (NBS), 2,2'-azobis(isobutyronitrile) / CCl4 / 0.67 h / Heating; Irradiation
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); pentan-1-ol; iodine; sodium; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
hydrogenchloride;
In
tetrahydrofuran; tetrachloromethane; acetic acid; benzene;
DOI:10.1021/jo00342a041
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 20 percent / benzene; acetic acid / 5 h / 80 °C
2: 99 percent / conc. HCl / acetic acid / 1 h / Heating
3: 66 percent / iodine / tetrahydrofuran; benzene / 3 h / 80 °C
4: N-bromosuccinimid (NBS), 2,2'-azobis(isobutyronitrile) / CCl4 / 0.67 h / Heating; Irradiation
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine;
hydrogenchloride;
In
tetrahydrofuran; tetrachloromethane; acetic acid; benzene;
DOI:10.1021/jo00342a041