Technology Process of C53H58(2)H5NO13Si
There total 7 articles about C53H58(2)H5NO13Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane;
at 40 ℃;
for 8h;
DOI:10.1002/jlcr.1870
- Guidance literature:
-
Multi-step reaction with 5 steps
1: formic acid / 2 h / 20 °C
2: triethylamine / dichloromethane / 0.5 h / 20 °C / Cooling with ice
3: 1H-imidazole / N,N-dimethyl-formamide / 8 h / 70 °C
4: dmap / chloroform / 2.5 h / 20 °C
5: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 8 h / 40 °C
With
1H-imidazole; dmap; formic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1870
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 8 h / 70 °C
2: dmap / chloroform / 2.5 h / 20 °C
3: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 8 h / 40 °C
With
1H-imidazole; dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane; chloroform; N,N-dimethyl-formamide;
DOI:10.1002/jlcr.1870