2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene

Base Information

• Chemical Name: 2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene
• CAS No.: 261907-35-1
• Molecular Formula: C₃₆H₄₄N₄Si₂
• Molecular Weight: 588.943
• Mol file: 261907-35-1.mol

Synonyms:2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene

Chemical Property of 2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene

There total 1 articles about 2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

diphenyl acetylene (501-65-5) + pentakis(dimethylamino)chlorodisilane (145700-15-8) → tris(dimethylamino)chlorosilane (13307-05-6) + 2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene (261907-35-1)

Guidance literature:

at 200 ℃; for 48h;

DOI:10.1016/S0022-328X(02)01142-7

Reference yield: 95.0%

2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene (261907-35-1) → 2,3,5,6-tetraphenyl-1,1,4,4-tetrachloro-1,4-disilacyclohexa-2,5-diene (37862-82-1)

Guidance literature:

With tetrachlorosilane; In diethyl ether; at 45 ℃; for 24h;

DOI:10.1016/S0022-328X(02)01142-7

Reference yield: 95.0%

2,3,5,6-tetraphenyl-1,1,4,4-tetrakis(dimethylamino)-1,4-disila cyclohexa-2,5-diene (261907-35-1) → 2,3,5,6-tetraphenyl-1,1,4,4-tetrabromo-1,4-disilacyclohexa-2,5-diene

Guidance literature:

With tetrabromosilane; In diethyl ether; at 45 ℃;

DOI:10.1016/S0022-328X(02)01142-7

upstream raw materials:

diphenyl acetylene

pentakis(dimethylamino)chlorodisilane

Downstream raw materials:

2,3,5,6-tetraphenyl-1,1,4,4-tetrachloro-1,4-disilacyclohexa-2,5-diene