C₂₄H₃₄N₂O₈S

Base Information

Chemical Name:C₂₄H₃₄N₂O₈S
CAS No.:1334173-69-1
Molecular Formula:C₂₄H₃₄N₂O₈S
Molecular Weight:510.609
Hs Code.:

C<sub>24</sub>H<sub>34</sub>N<sub>2</sub>O<sub>8</sub>S

Synonyms:C₂₄H₃₄N₂O₈S

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Chemical Property of C₂₄H₃₄N₂O₈S

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Technology Process of C₂₄H₃₄N₂O₈S

There total 19 articles about C₂₄H₃₄N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1334173-68-0
C₂₈H₄₂N₂O₁₀S

: 1334173-69-1
C₂₄H₃₄N₂O₈S

Guidance literature:: With trimethylsilyl bromide; In dichloromethane; at 0 ℃; for 18h; Inert atmosphere;
DOI:10.1002/anie.201103550

Reference yield:

: 1334173-57-7
C₂₅H₃₀O₃Si

: 1334173-69-1
C₂₄H₃₄N₂O₈S

Guidance literature:: Multi-step reaction with 15 steps

1.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

1.2: 13 h / -78 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.1: dicobalt octacarbonyl / toluene / 1.5 h / 20 °C / Inert atmosphere

3.2: 12 h / 100 °C

4.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

5.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

7.1: sodium hydrogencarbonate / 1,2-dichloro-benzene / 10 h / 170 °C / Inert atmosphere

8.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere

8.2: -78 - 20 °C / Inert atmosphere

9.1: dimethylsulfide borane complex / tetrahydrofuran; dimethylsulfide / 12.5 h / 0 °C / Inert atmosphere

9.2: 10 h / 0 °C / Inert atmosphere

9.3: NaBO₃*4H₂O / 4 h / 20 °C / Inert atmosphere

10.1: triethylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

11.1: dmap / pyridine; dichloromethane / 0 - 20 °C / Inert atmosphere

12.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

13.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

14.1: triphenylphosphine; diethylazodicarboxylate / toluene / 14 h / 70 °C / Inert atmosphere

15.1: trimethylsilyl bromide / dichloromethane / 18 h / 0 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium borohydride; n-butyllithium; dicobalt octacarbonyl; borane-THF; trimethylsilyl bromide; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hexamethyldisilazane; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; diethylazodicarboxylate; In tetrahydrofuran; pyridine; dimethylsulfide; hexane; dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; toluene; mineral oil; 3.1: Pauson-Khand reaction / 3.2: Pauson-Khand reaction / 14.1: Mitsunobu reaction;
DOI:10.1002/anie.201103550

Reference yield:

: C₂₆H₃₄O₄Si

: 1334173-69-1
C₂₄H₃₄N₂O₈S

Guidance literature:: Multi-step reaction with 16 steps

1.1: pyridinium p-toluenesulfonate / isopropyl alcohol; toluene / 28 - 80 °C / Inert atmosphere

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2.2: 13 h / -78 °C / Inert atmosphere

3.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: dicobalt octacarbonyl / toluene / 1.5 h / 20 °C / Inert atmosphere

4.2: 12 h / 100 °C

5.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

6.1: borane-THF; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

7.1: sodium hydride / tetrahydrofuran; mineral oil / 0 - 20 °C / Inert atmosphere

7.2: 0 - 20 °C / Inert atmosphere

8.1: sodium hydrogencarbonate / 1,2-dichloro-benzene / 10 h / 170 °C / Inert atmosphere

9.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C / Inert atmosphere

9.2: -78 - 20 °C / Inert atmosphere

10.1: dimethylsulfide borane complex / tetrahydrofuran; dimethylsulfide / 12.5 h / 0 °C / Inert atmosphere

10.2: 10 h / 0 °C / Inert atmosphere

10.3: NaBO₃*4H₂O / 4 h / 20 °C / Inert atmosphere

11.1: triethylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

12.1: dmap / pyridine; dichloromethane / 0 - 20 °C / Inert atmosphere

13.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

14.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

15.1: triphenylphosphine; diethylazodicarboxylate / toluene / 14 h / 70 °C / Inert atmosphere

16.1: trimethylsilyl bromide / dichloromethane / 18 h / 0 °C / Inert atmosphere

With N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium borohydride; n-butyllithium; dicobalt octacarbonyl; borane-THF; trimethylsilyl bromide; dimethylsulfide borane complex; tetrabutyl ammonium fluoride; pyridinium p-toluenesulfonate; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium hydrogencarbonate; potassium carbonate; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium hexamethyldisilazane; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; diethylazodicarboxylate; In tetrahydrofuran; pyridine; dimethylsulfide; hexane; dichloromethane; N,N-dimethyl-formamide; 1,2-dichloro-benzene; isopropyl alcohol; toluene; mineral oil; 4.1: Pauson-Khand reaction / 4.2: Pauson-Khand reaction / 15.1: Mitsunobu reaction;
DOI:10.1002/anie.201103550