C₂₈H₂₉NO₇

Base Information

Chemical Name:C₂₈H₂₉NO₇
CAS No.:1280608-53-8
Molecular Formula:C₂₈H₂₉NO₇
Molecular Weight:491.541
Hs Code.:

C<sub>28</sub>H<sub>29</sub>NO<sub>7</sub>

Synonyms:C₂₈H₂₉NO₇

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Chemical Property of C₂₈H₂₉NO₇

Chemical Property:

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Technology Process of C₂₈H₂₉NO₇

There total 5 articles about C₂₈H₂₉NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1280608-52-7
C₃₀H₃₃NO₇

: 1280608-53-8
C₂₈H₂₉NO₇

Guidance literature:: With water; pyridinium p-toluenesulfonate; In 1,4-dioxane; at 70 ℃; for 12h;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-49-2
C₂₁H₂₁NO₆

: 1280608-53-8
C₂₈H₂₉NO₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 14 h / 40 °C

2.1: sodium tetrahydroborate / tetrahydrofuran; methanol / 0 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

3.2: 2.5 h / 20 °C

4.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

5.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; Oxone; sodium tetrahydroborate; C₁₃H₂₀O₉; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; methanol; Dimethoxymethane; dichloromethane; water; acetonitrile; mineral oil; 4.1: Shi epoxidation;
DOI:10.1002/anie.201006528

Reference yield:

: 1280608-50-5
C₂₃H₂₇NO₆

: 1280608-53-8
C₂₈H₂₉NO₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0 °C

1.2: 2.5 h / 20 °C

2.1: Oxone; C₁₃H₂₀O₉; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate / Dimethoxymethane; water; acetonitrile / 24 h / 0 °C / pH 6 / aq. phosphate buffer

3.1: water; pyridinium p-toluenesulfonate / 1,4-dioxane / 12 h / 70 °C

With Oxone; C₁₃H₂₀O₉; water; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; sodium hydride; potassium carbonate; In tetrahydrofuran; 1,4-dioxane; Dimethoxymethane; water; acetonitrile; mineral oil; 2.1: Shi epoxidation;
DOI:10.1002/anie.201006528