3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate

Base Information

Chemical Name:3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate
CAS No.:1224598-11-1
Molecular Formula:C₁₆H₂₂N₃O₄PS
Molecular Weight:383.408
Hs Code.:

Synonyms:3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate

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Chemical Property of 3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate

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Technology Process of 3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate

There total 1 articles about 3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 874493-33-1
pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate

: 3466-32-8
4-bromoohenyl methyl sulfone

: 1224598-11-1
3-[4-(methylsulfonyl)phenyl]pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate

Guidance literature:: pyridin-2-yl N,N,N',N'-tetramethyldiamidophosphate; With 2,2,6,6-tetramethylpiperidinylmagnesium chloride lithium chloride complex; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

With zinc(II) chloride; In tetrahydrofuran; at -40 ℃; for 0.25h; Inert atmosphere;

4-bromoohenyl methyl sulfone; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; ruphos; In tetrahydrofuran; at -40 - 25 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/ol100453x