Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

Base Information

Chemical Name:Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside
CAS No.:155195-17-8
Molecular Formula:C₅₂H₇₈O₂₅Si₂
Molecular Weight:1159.35
Hs Code.:

Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

Synonyms:Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

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Chemical Property of Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

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Technology Process of Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

There total 3 articles about Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 155194-86-8
Methyl 2-O-benzoyl-6-O-dimethylthexylsilyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

: 440-03-9
2,3,6-tri-O-acetyl-4-O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranosyl fluoride

: 155195-17-8
Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

Guidance literature:: boron trifluoride diethyl etherate; In dichloromethane; for 2.5h; Ambient temperature;

Reference yield:

: 75156-19-3
Methyl 3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

: 155195-17-8
Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: imidazole / dimethylformamide / 1 h / Ambient temperature

2: pyridine / 16 h / Ambient temperature

3: 61 percent / BF₃*Et₂O / CH₂Cl₂ / 2.5 h / Ambient temperature

With pyridine; 1H-imidazole; boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 155194-85-7
(1R,3S,4R,4aR,9aR)-1-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxymethyl]-6,6,8,8-tetraisopropyl-3-methoxy-tetrahydro-2,5,7,9-tetraoxa-6,8-disila-benzocyclohepten-4-ol

: 155195-17-8
Methyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->4)-O-(2,3,6-tri-O-acetyl-β-D-glucopyranosyl)-(1->6)-2-O-benzoyl-3,4-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 16 h / Ambient temperature

2: 61 percent / BF₃*Et₂O / CH₂Cl₂ / 2.5 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;